有機化学実験 Lab Work in Organic Chemistry



日程


6/8(木)

13:00-13:20 スタッフ・TA紹介と有機化学実験の諸注意

13:20-14:20 実験ノート,レポートの書き方講義,安全対策(危険物、廃棄物の処理)講義

14:30-14:50 1. ヘアピンリボザイムの合成と反応 実験講義

14:50-16:10 器具の点検


6/12(月)-6/15(木)*2  1. ヘアピンリボザイムの合成と反応

6/19(月)–6/22(木)*3  2. 基本操作

6/26(月)–7/3(月)*4  3. β-ケトエステルの反応とWittig反応

7/4(火)–7/11(火)*5  4. 縮合反応とDiels-Alder反応

7/2(水)–7/18(火)  5. 未知試料の構造決定と誘導体合成(1)


7/19(水)

13:00-13:40  文献調査講義・出題

13:45-14:45  文献検索 SciFinder講習会

14:45-16:10  片付け,掃除


9/25(月)13:00  文献調査 中間レポート提出期限


9/25(月)-9/27(水)*6  5. 未知試料の構造決定と誘導体合成(2)

9/28(木)–10/5(木)*7  6. Grignard反応とFriedel-Crafts反応

10/10(火)–10/18(水)  7. 芳香族化合物の反応


10/18(水)13:00  文献調査 最終レポート提出期限


10/19(木)  片付け,掃除


*:13:00より,数字で示す単元の実験講義を行う



Schedule


Thu, 6/8

13:00-13:20  Introduction of staff members and TAs in charge, general instructions

13:20-14:20  Lecture on laboratory notebooks and reports

        Lecture on safety (handling hazardous substances and chemical waste)

14:30-14:50  Lecture on Unit 1. Synthesis and reactions of hairpin ribozyme

14:50-16:10  Inspection of instruments


Mon, 6/12 - Thu, 6/15*2  1. Synthesis and reactions of hairpin ribozyme

Mon, 6/19 – Thu, 6/22*3  2. Basic operations

Mon, 6/26 – Mon, 7/3*4  3. Reactions of -ketoesters and Wittig reaction

Tue, 7/4 – Tue, 7/11*5  4. Condensation and Diels-Alder reaction

Wed, 7/2 – Tue, 7/18  5. Structure determination of unknown sample and synthesis of derivatives (1)


Wed, 7/19

13:00-13:40  Lecture and assignment of literature review

13:45-14:45  Training on SciFinder

14:45-16:10  General cleanup


Mon, 9/25, 13:00 Deadline of literature survey intermediary report


Mon, 9/25 - Wed, 9/27*6  5. Structure determination of unknown sample and synthesis of derivatives (2)

Thu, 9/28 – Thu, 10/5*7  6. Grignard and Friedel-Crafts reactions

Tue, 10/10 – Wed, 10/18  7. Reactions of aromatic compounds


Wed, 10/18, 13:00  Deadline of literature survey final report


Thu, 10/19  General cleanup


*Lecture on the experiment unit indicated by the figure starts at 13:00.